Distillation

General Info


1)  Condenser

2)  Reflux ratio

3) Distillation columns 

     McCabe-Thiele Diagrams Part 1/Part 2 

     Murphee efficiency calculations 

     Txy diagrams

4) Reboiler


Lab Info



1) Trace water line to main valve on wall

2) Water valve to control water to condenser

3) Sample valve for tops

4) Sample valves for bottoms

5) Vapor effluent tube to hood

Main Console

1) On/off switch (O indicates "on")

2) Display for amount a reflux cycle occurs

3) Reflux control method

4) Display for amount of power going to reboiler 

5) In manual mode, controller for reboiler power

6) Reboiler power control method

7) Temperature displays

8) Thermocouple selection for display

Software

1) "Go" button to start recording the data

2) Table button where temperature data is found

3) Setup button to set sample mode

4) Thermocouple data 

5) In I/O Port mode, amount of reboiler power

6) Save button for saving data to flash drive

Water Valve

Water valve location on South wall

Verify water is running into sink before turning on reboiler